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More on this later. Also, does anyone have a good article on the Tianjin incident? I know there's a lot of sodium cyanide in the destroyed warehouse, but that doesn't explain the initial explosion. Nomination for the top 5 of the "Hiss and Ping" analytical techniques descriptions. It's taken almost two months, but finally, below are the entries for the contest for the funniest, most accurate description of an analytical technique.
Vote in the comments for your favorites. The top 5 vote winners will be judged by our panel of analytical chemists:. Turn on a radio, and the atoms sway to one side while dancing with each other. Turn off the radio and watch as the dipoles in the atoms dance back. Repeat until you can draw it yourself. Tune into the right frequency and you'll learn something about a specific situation that can also teach you something broad and fundamental about the environment in which it occurs.
NMR is like radio-frequency-based molecular Twitter. Hit your sample with one short, pointed "statement" on a given frequency and then sit back listen to all the related nuclear opinions that come back at you. Fair warning: lot of it will just be noise. AnonPM: "Sum frequency generation, where a surface becomes a Thunderdome: two frequencies enter, one leaves. Evil: Alright, here's the plan.
Here's the plan. Back in the 60's, I had a mass spectrometry machine that used, in essence, a sophisticated laser beam which we called an "Ninja Assassin. By timing the "Speed" at which ions "Race" to the detector we can determine their mass with incredible precision.
Evil: Any ways, the key to this plan is controlling the rising gas. Like "Jupiter Ascending' it can quickly overload detector without proper safeguards. Because overall futuristic flair, and the polish source of "The Matrix", we shall call the device the Wachowski Starship.
Evil: Right, people you have to tell me these things, okay? I've been frozen for thirty years, okay? Throw me a frickin' bone here! I'm the boss! Need the info. You shine an IR source spectrometer or remote control at your sample chemical or TV , and the signal that you get in return doesn't usually tell you anything useful that you don't already know.
The carrier gas sweeps the mixture over hot metal surfaces, where the compounds of interest degrade or rearrange, into a column where they are separated. Molecules that exit the column i. Senior citizens will say computerized data system. The retention times of compounds may change as the stationary phase changes due to deposition of residues from dirty samples and reaction with oxygen from leaks.
For compounds with similar mass spectra e. This usually only happens when data are to be published or the sample is a PT sample. You see, back in the s, gents in well-tailored suits with big glasses posed next to giant, room-filling machines capable of only a fraction of today's tablet computers' power. These men - and they were always men, then - would place thin glass tubes of their molecule into relatively misshaped magnetic fields and send in specific radio waves, hoping out the other side to see their recorder pens transcribe a forest of little inky peaks.
Now, this worked fine if you wanted ALL the information about each and every proton in the molecule, but what if all you wanted to do was count carbons? Sending in radio waves tuned to carbon sent back little patterns of 2, 3, 4 or more peaks, depending on how many Hs were bound to each C.
Too much info! Instead, if you blast all the protons with one high-powered radio pulse, their coupling to C falls apart, and you can sneak in a carbon-only pulse just afterwards. Et voila! Simple, single peaks shifted to match the chemical environment of where you found 'em in the molecule. Carbons next to things that tug on their electrons are on your left. Easy as pie. This applies to multiple spectroscopy techniques. ForensicToxGuy: "Time of flight mass spectrometry is akin to a foot race between skinny kids and heavier kids.
They all start approximately at the same starting line. The gun goes off and the race starts. The lighter kids travel faster and the heavier kids are slower through the race course. The skinnier kids get to the finish line first while the heavier kids finish later.
You take an irreplaceable archaeological artifact, smash it, pour acid on it, burn it, then catapult any remains as fast as current technology will allow. You start vertical, but then get excited and end up horizontal. Then you roll around a few times Your act consists of you holding a fairly large butterfly net, ready to catch what ever miniature clowns run through that doorway.
But the mini clowns don't actually run in, they are actually being shot out of a cannon. Through the door. Into your net. But your cannon is kinda crappy so if the clown is too big, it just kinda plops out of the cannon and doesn't make it very far Probably won't even make it through the doorway.
But if the clowns are small, they get launched from the cannon with impressive speed Probably too much speed so that when you try to catch them, they rip the net right out of your hands and keep going on their trajectory straight into the audience, perhaps into that section of nuns.
It turns out, for the trick to work allowing the audience to see your daring clown capture, you need clowns of just the right size. Since you don't have a scale, the only way to find clowns of the right size is trial and error. Poison Ivy League : "1HokeyPokey. Elemental Analyfish II:. Labels: blog contest , fun. Irvine, CA: This information analyst position with Allergan is fascinating, in that it doesn't require a master's in library science degree; instead it asks for a Ph.
LinkedIn shows positions for the job title "chemist", 75 positions for "analytical chemist", 31 for "research chemist", 12 for "organic chemist", 5 for "synthetic chemist" and 3 for "medicinal chemist. Job post: director of life sciences, ACSH job description revised. Friend of the blog Josh Bloom sends a revised version of this job description to the inbox:. Thursday, August 20, Why Dr. My thoughts on Dr. From an online perspective, it's especially silent.
I don't run in academic circles anymore not that I really ever did , so it's hard to say what kind of conversations about Prof. Harran's or UCLA's culpability have taken place during group meetings and the like. New details on the incident: I'd like to hear more details that Prof. Harran asked her to perform the tBuLi syringing without the appropriate equipment what equipment would that be?
Certainly one could unpack a cannula and a graduate cylinder. Personally, I think it's more likely that Prof. Harran asked her to do the syringe transfers and that he never thought that anything bad could have taken place. How would someone even begin to pressure the board to act? I can't imagine that they ever would have. They seem to shy away from that sort of controversy.
While I agree that funding is certainly the only true coercive power that the NIH has over the universities, I repeat the same criticism of this potential policy that I have long made when it was brought up by Beryl Benderly, back in : How is it possible to accurately judge a PI's safety record? How do you get accurate data? How could you possibly avoid the inevitable sweeping under the rug of near-misses and actual safety incidents in order for professors, postdocs and students to continue to get funding?
If I was a graduate student that had an accident and I knew that going to the emergency department for stitches meant that I'd be jeopardizing the future funding of my PI and my coworkers, I'd be sewing cuts up myself to avoid the potential damage to my career. Apart from my policy critique, I believe that Dr. Sangji has a fundamental misunderstanding of the ACS and its relationship to the academic community.
It's an organization that derives most of its Society-wide funding from ACS Publications, a publishing house which gets its work product, for free, in raw form from the academic community and then charges those same academics for access to its journals. Why would ACS ever decide to jeopardize this relationship over what is in the ACS headquarters' eyes, I suspect an internal employee safety dispute of its chief customer? If there is one thing that I have learned over the past 6 years of watching the American Chemical Society attempt to deal with the mess that is chemist employment in the United States, it is this: it does not have tremendous power.
While I wish that it held power over the chemical industry, it does not. While I wish it held power over academic chemistry, it does not. In fact, I would say that the only actual power it holds is its ability to extract revenue from universities via its subscriptions.
However, how much sway does it have with NIH? Who does Francis Collins listen to more? Can anyone point to a single example in the last 10 years where the ACS has had any effect on governmental action at the state or federal level? Here's my suggestion for how Dr. Pressing her sister's memory on each and every member of the American Chemical Society is tremendously important from a cultural perspective, but in this nation of laws, it's Congress that holds the true power.
Labels: Sheri Sangji. Wednesday, August 19, Dr. Busy today, but I did want to take note that Dr. This is the third best ratio since then, I think 3. This is the 3rd largest absolute number of jobs Boston , Denver Labels: ACS job fair white board. Tuesday, August 18, Missouri cuts health care subsidies for graduate students with less than 24 hours notice. A very interesting little story coming out of the University of Missouri.
Labels: dumb grad school theories. I'd cut that down by 14, considering that's how many were posted by ACS. Juicing the stats? Maybe a little. Lubbock, TX: Texas Tech University is looking for an assistant professor of chemistry , specializing in "experimental soft matter.
Middlebury, VT: Middlebury College is looking for a laboratory instructor for a 3. Stanford, CA: Stanford has 2 openings for staff radiochemists ; B. Labels: ivory filter flask. Labels: acs career fairs , ACS job fair white board. They have been doing a fantastic job covering the negative effects of the Great Recession on the ACS' member chemists.
I do not understand why this choice was made, but regardless of the reason, the effect is the same. Labels: cen inside baseball. They have to meet 3 criteria: tenure-track faculty positions with anticipated start dates in in chemistry departments or with a focus on chemistry at institutions in the United States or Canada Obviously, there will be interesting edge cases as to what gets included here. Click here to see the list of current positions at ChemBark; here is the current list in downloadable spreadsheet format.
Labels: dumb employment theories. A sobering aspect of the Internet and chemistry jobs. Owing to their limited venture capital funding, most small biotech companies in California work on only one compound, and if that candidate fails to advance to clinical trials, as is usually the case, then everyone at the company is laid off.
But if the compound beats the odds and succeeds in progressing to the clinical trial stage, the entire early discovery lab is laid off anyway. Compared with betting on a single candidate, the pursuit of multiple projects at once offers a much better chance of success, and that means everyone in the company—10 people or so, at the moment—can keep their jobs, Wu says.
Currently, he notes, the company has a few candidates undergoing Phase II trials. VM develops oral drug candidates to treat central nervous system disorders, cancers, and other diseases. The firm relies on Chinese contractors to not only conduct laboratory work but also to manufacture small batches of its drug candidates for U. I don't work in the virtual space enough to understand how well this works out for companies; I guess it's about embracing the instability, sigh.
A survey on how chemists use the Internet. I love this Martyn Poliakoff piece on the periodic table and the Web. Carolyn Bertozzi talks about online serendipity. Derek Lowe's comments on the chemistry blogosphere and the literature. Here's Paul Bracher's piece on ChemBark. Comments on the job market by some rando.
This story on new beryllium safety standards by Andrea Widener is interesting - I had no idea that it was used outside of nuclear weapons. Bethany Halford covers work by the Buchwald group on embedding air-unstable compounds in paraffin capsule. It's so simple, I feel dumb for not having thought of it before. Friday, August 14, Boston open thread. Anyone want to plug anything at ACS Boston? Friends of the blog Raychelle Burks and Matt Hartings among others will be speaking on a panel on Monday as well.
There's a University of Minnesota-run polymer chemistry symposium on Tuesday. Wish I could be there! Maybe in San Diego? If Chemjobber readers decide to have a get-together in the comments to the post, do take a picture and send it. Update: A few chances to meet fotb Organometallica. Also, I understand there will be a chemistry Twitter meetup on Monday night. Labels: acs boston This is an annual science fiction convention; prominent online science communicator Raychelle Burks has been putting on the Zone, where children and adults are invited to interact with hands-on science demonstrations and the like.
It's a lot of fun and I have enjoyed participating in it. We do a lot of fundraising for the Zone for supplies, etc. One of the things we're supposed to do is Acts of Whimsy when we meet certain fundraising goals. Hope you enjoy.
If you feel like donating, here's a link. Labels: fun , geek girl con , podcast. Scientists Invent Bottleneck-Destroying Machine. Chemjobber News It sounds like something out of Medicine Man, but it's true. In a study published today in the journal Science , researchers have announced the discovery of the "Holy Grail" of chemistry: a machine that eliminates bottlenecks. Textbooks will need to be shredded as the research challenges the long-held notion that bottles require necks, or that any container requires a narrower opening.
We have destroyed all known bottlenecks. They're gone. That Diet Coke bottle you had in your office? Get it within two feet of our machine and it'll be a cup. Aldrich 4 liter bottles are gonna be jars from here on out. The breakthrough is sure to be heralded as good news for managers who love to prattle on about "de-bottlenecking".
But some will be asking questions about the need for this research in our increasingly open-top, all-access society. Smith, who was not involved with the research, says that the results are "intriguing" but there is not yet enough information to draw any conclusions. Come up with your own science story here at Buzzfeed.
Okay, so this one's a little embellished. Thursday, August 13, A clarifying graph of ages of laid-off Intel employees. Age distribution of a July layoff of Intel employees Credit: Oregonlive. Apparently, the employees were shown a graph of who was laid off as part of federal law? The actual data XLS can be downloaded if you click through. I don't seem to remember similar graphs coming out of the period of layoffs in pharma - I wonder why? Sure looks like the upper end of the age distribution took the biggest hit, though, doesn't it?
The average age of an Intel employee in the United States is Optional: include an answer key. Stray Animal: Think of the life of a stray cat or dog and write about that. Fireworks : Do they inspire you or do you not like the noise and commotion? Frozen: Write about a moment in your life you wish you could freeze and preserve. Did you keep that promise? Choose one of them to write a strong essay on love. There are several essay categories presented.
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Get the sheridan center for every day discuss teaching resources for any liability. Short precise keywords, m. Department of Veterans Affairs. Here's how students can access Education. Choose which type of app you would like to use. To use our web app, go to education. Or download our app "Guided Lessons by Education. Student Code. Ok, Got it. School and Academics. Test Preparation. Collect This Article. Download Article. Short Answer Short answer questions usually ask students to list , name , define , or identify.
Therefore, review your notes and try to anticipate what information falls under those categories. For instance, if you're studying World War II, try identifying the causes of the War, defining each country's stance, and listing the repercussions. Thinking ahead and approaching a topic from the right angles can make all the difference. It may sound obvious, but using flashcards to study the material really does work.
Put key terms, dates and concepts on one side and the answers on the other. The process of writing the information down on the cards, reading the cards, and being quizzed with the cards helps commit the information to memory.
During the test, underline key words to focus your attention on what is being asked. Identify these points and put them in your outline. If you run out of time and don't explain all of the points on your outline, write down the points in your outline and add a note saying that you ran out of time.
You may get partial credit for your effort. Taking a test doesn't have to be a dreadful experience. Practicing your test-taking skills will help you manage the anxiety that often accompanies tests. Good test-taking skills will not guarantee that you will get an "A" on every test, but they will ensure that your test score reflects what you really know.
Free Essay: The test taking lessons have helped me learn more about having good strategies for a test. I feel that with these lessons learned I can have more. Unfortunately, it's still one of the biggest test taking mistakes students make. Before answering an essay question, thoroughly read the instructions. Do not jump. Green, Gordon W. Getting Straight A's. Secaucus, New Jersey:. Lyle Stuart, Inc. Kesselman-Turkel, Judi and Peterson, Franklynn. Test Taking Strategies. Chicago, Illinois: Contemporary Books, Inc.
Library Reference Search. Please note that this site is privately owned and is in no way related to any Federal agency or ERIC unit. Further, this site is using a privately owned and located server. This is NOT a government sponsored or government sanctioned site. You can always go back and change things later if needed, but a few quick answers can get the ball rolling. Everyone else is scribbling away? Pay attention to your own test and pace, and forget about the other students in the room.
Realizing that time is almost up and there are lots of test questions left can make it hard to do anything useful in those final minutes. Stay on pace by scoping out the whole test before getting started. Deep breathing can slow down a beating heart or a racing mind, so practice these techniques at home. The very act of concentrating on breathing and thinking can biometrically alter those anxious feelings. If you need a confidence boost, try a session with an online tutor.
From PhDs and Ivy Leaguers to doctors and teachers, our tutors are experts in their fields, and they know how to keep your anxiety at bay. Take a few minutes at the start of the exam period to read and think about each question. Make sure that you read the instructions carefully: know from the start how many questions you're supposed to answer and how long your answers are expected to be. For standardized tests such as the SAT or the ACT , make sure that you visit the test websites well before the day of the test so that you can read all instructions ahead of time.
Read the topic several times, looking for key words that indicate how you should develop and organize your essay:. Calculate the time you have in which to write the essay, and set up a schedule. While working under a one-hour time limit, for instance, you might designate the first five or ten minutes for discovering ideas and planning your approach, the next forty minutes or so for writing, and the last ten or fifteen minutes for revising and editing.
Or you might allot a shorter period to the initial drafting and devote more time to revising the essay. In any case, plan a realistic schedule--one based on your own writing habits--and then stick to it. Reread and review those areas in the text where there is limited understanding and comprehension. Carefully read the question.
Break the question into parts so you know what you need to answer for full credit. Take the time to create an outline on your answer sheet so that even if you don't complete the essay the professor can see where you were going and may give you points. Although you are taking a few minutes away from answering the essay, it will increase your chances for a more coherent answer with examples that flow and an essay that makes sense.
Use the parts of the essay to help create the outline - this will help with organization and keep you focused on topic. Follow your outline and begin the essay. Write straight through and do not vary from the outline. You took the time to write it out so trust it. If you try to change the direction of your essay, you end up with arrows etc.
The easier your essay is to read and the better it flows, the easier it will be for your professor to follow your train of thought thus a better grade. Reread the directions and make sure you answered the entire questions. And if you still have time, reread your essay and correct spelling and grammar errors. Taking the exam is only the first part to knowing what you know.
The second part comes with the handing back of the exam. At this time you have the prime opportunity to see what you knew and learn what you didn't. You should always go back and find out why you missed particular questions, what type of questions they were, did you answer the whole questions or only part, then definitely find the correct answer and write it out so you know you know it.
This is especially useful if you will be taking a comprehensive final. Make sure you talk with the professor about how you can improve in a particular area or ask why they worded the question the way they did. Most students experience some level of anxiety but it is when it interferes with test performance that it is deemed excessive and labeled test anxiety.
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An essay is a representation of your understanding of a problem and therefore you should take care of its presentation to make a good first impression on your tutor. Most of written assignments are required to be done in typewriting, for sometimes it is difficult to read handwriting.
Poor essays are often merely a patchwork of quotations stitched together by the briefest of comments, and it is a mistake to leave quotations hanging in mid-air, as it were, without comment or explanation. Quotations need to be framed. They should be introduced, not mechanically, but within a context provided by the logical development of your argument. See Example 1 at the end of this guide. This is often likely to be the case as there is really little point in including 'bland' quotations in your essay.
You may want to gloss, explain, qualify or modify the quoted words, or you may have included quotations whose assumptions or arguments you strongly disagree with. The latter case can be useful, if handled well. Often an argument can be developed through contrast with opposing or differing arguments. This tactic in essay construction also displays independent thinking in that it demonstrates that you have not unthinkingly accepted and believed everything you have read.
One final point on quotations: do not plagiarise. Using other people's work without saying so is a serious crime. Tutors have read widely on the subjects you will be writing on and are very likely to recognise when you are plagiarising. If you use other people's ideas and words they have to be acknowledged through proper footnoting and referencing. See Example 2 at the end of this guide. Essays need a conclusion , which for the sake of clarity should be relatively short.
It is generally best not to include new ideas or new material in your concluding comments, particularly since many people think that a conclusion should be a synthesis of the prior arguments. You may, however, point to alternative conclusions or arguments, or briefly suggest areas of interest that have not been dealt with directly by the essay. People often get the wrong idea about conclusions and believe that this is the place to state firm convictions, and that a conclusion has to make a stand and come down on the side of one argument or another.
This can be the case but it is not necessarily so.
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